Supplier of European Chemical Raw Materials
European Technologies Incorporated, 4835 West 31st Avenue, Denver, Colorado 80212, USA
               Phone: 303-433-1816, Fax: 303-455-2172, e-mail: info@etichem.com
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European Technologies Inc.
4835 West 31st Avenue
Denver, CO 80212, USA
Phone: 303-433-1816
Fax: 303-455-2172
e-mail: info@etichem.com
METHYSERGIDE MALEATE
Technical specifications
Product nr.: CZ13-0110
Ordering: to obtain pricing, to order, or for additional information, please call: European Technologies Inc. at 303-433-1816, or e-mail to mfranta@etichem.com
Shelf life:  2 years when stored properly.
Packaging: Per customer request.
Storage conditions: Store cool and dry. 
Methysergide maleate

Product name:

Methysergide Maleate
   

Empirical formula:

C21H27N3O2 . C4H4O4

Molecular weight:

469.5

CAS:

[129-49-7]

Description:

White to yellowish white or reddish white, crystalline powder.

Identity

  

    IR:

Complies

    TLC:

Complies

Specific rotation:

35.0 to 45.0°

pH of the solution:

3.4 to 4.7

Loss on drying:

NMT 7.0 %

Impurities

  

    Methyl ergometrine by HPLC:

NMT 1.0 %

    Methysergidine by HPLC:

NMT 0.5 %

    Other individually:

NMT 0.1 %

    Total amount of impurities:

NMT 2.0 %

Organic volatile impurity

  

    Dichloromethane:

NMT 100 ppm

Residual solvents

  

    Ethanol:

NMT 3,000 ppm

    Methanol:

NMT 1,000 ppm

    Other individually:

NMT 200 ppm

Assay

  

    Recalculated on anhydrous basis:

97.0 – 103.0 %